Hydrometallurgical Synthesis of pure zincite (ZnO) powder from dead zinc carbon batteries for use in the manufacturing of antimicrobial products

Authors

  • Ibrahim Kuranga Ayinla Department of Industrial Chemistry, University of Ilorin, P.M.B. 1515, Ilorin-240003, Nigeria
  • Seyi Ebun Adeboye Biotechnology Department, National Biotechnology Development Agency, Abuja, Nigeria
  • Mufutau Abiodun Salawu Department of Physics. University of Ilorin, Ilorin, Nigeria
  • Asim Abdallah Mohammed Physics Department, Faculty of Education, University of Zalingei, Sudan
  • Abdullahi Alafara Baba Department of Industrial Chemistry, University of Ilorin, P.M.B. 1515, Ilorin-240003, Nigeria
  • Islamiya Oluwatosin Ali Department of Industrial Chemistry, University of Ilorin, P.M.B. 1515, Ilorin-240003, Nigeria
  • Abdulmajeed Mualiyu Department of Industrial Chemistry, University of Ilorin, P.M.B. 1515, Ilorin-240003, Nigeria
  • Bankim Chandra Tripathy CSIR - Institute of Minerals and Materials Technology, Bhubaneswar-751013, India

DOI:

https://doi.org/10.37134/ejsmt.vol12.2.3.2025

Keywords:

Hydrometallurgy, Kinetics, Metallurgy, Powder Technology, X-ray, Zincite

Abstract

The conversion of waste materials in our environment into useable chemical products is a popular issue these days. Here, we report on the production of zincite powder using a very simple hydrometallurgical method. Within two hours, 92.23% of the original 10 g/L SZCB reacted at ideal leaching conditions (2.5 mol/L HCl, 80°C). The result predicted the diffusion model as rate determining step, with calculated Ea of 28.53 kJ/mol. The precipitated hydroxide was calcined to produce pure zincite powder of yield 85.2%. Analyses using X-ray diffraction (XRD) and scanning electron microscopy (SEM) revealed that the high purity ZnO existed as a flower-like spherical aggregation and antimicrobial testing was later carried out to be reported in part B of the research.

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Author Biography

  • Ibrahim Kuranga Ayinla, Department of Industrial Chemistry, University of Ilorin, P.M.B. 1515, Ilorin-240003, Nigeria

    Biotechnology Department, National Biotechnology Development Agency, Abuja, Nigeria

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Published

2025-10-23

How to Cite

Ayinla, I. K., Adeboye, S. E., Salawu, M. A., Mohammed, A. A., Baba, A. A., Ali, I. O., Mualiyu, A., & Tripathy, B. C. (2025). Hydrometallurgical Synthesis of pure zincite (ZnO) powder from dead zinc carbon batteries for use in the manufacturing of antimicrobial products. EDUCATUM Journal of Science, Mathematics and Technology, 12(2), 36-42. https://doi.org/10.37134/ejsmt.vol12.2.3.2025