Dielectric and Spectroscopic Evaluation of Specialty Coffee Acidity, Moisture, and Oxidation
DOI:
https://doi.org/10.37134/jsml.vol14.1.4.2026Keywords:
Microwave non-destructive testing, Dielectric permittivity, FTIR spectroscopy, Coffee quality, Correlation analysisAbstract
This article presents Microwave Non-Destructive Testing (MNDT) as a non-invasive method of evaluating specialty coffee quality by measuring dielectric permittivity at X-band frequencies (8-12 GHz). The moisture content, degree of oxidation, and acidity (pH) of light, medium, and dark roasted single-origin Arabica beans were examined during a 30-day resting period after roasting. Reference standards were analysed with Fourier Transform Infrared (FTIR) (400–4000 cm⁻¹) and calibrated pH meters. The highly negative correlation of dielectric permittivity with acidity (r = -0.979, ρ = -0.963, p < 0.001) yielding −0.963 and −0.979 Pearson and Spearman correlations is strong evidence that, of all the sensory qualities attributed to the specialty coffee, the most salient, the acidity, can be intravenously measured with great speed and accuracy. The correlations of moisture (r = 0.612, p = 0.012) and oxidation (r = 0.541, p = 0.028) suggest some degree of added dielectric sensitivity. However, the sensitivity to increased complexity of the coffee matrix from roasting is more relevant. The implications of this work are significant to food science and underscore the need to bridge siloed disciplines of physics and chemistry, demonstrating that microwave non-destructive testing (MNDT) is useful and non-invasive as a generalised substitute to the multitude of destructive methods in quality assessment. Its compliments the existing cupping method of application to the coffee industry, coupled with its improvement upon existing multivariate methods, indicates well for sustainable quality assessment.
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References
Adnan A, von Hörsten D, Pawelzik E, Mörlein, D. (2017). Rapid prediction of moisture content in intact green coffee beans using near infrared spectroscopy. Foods, 6(5), 38. doi:10.3390/foods6050038
Ahmad Lu ai Waez Awang, Ihsan Mohd Yassin, Mohd Khairil Adzhar Mahmood, Megat Syahirul Amin Megat Ali, Fairul Nazmie Osman, Michael Tan Kwan Yeow, Farzad Eskandari, Azlan Salim, & Zuhani Ismail Khan. (2023). Intelligent method for classifying the freshness of coffee. 2023 IEEE Symposium on Wireless Technology and Applications, 115-122. doi:10.1109/ISWTA58588.2023.10249522
Astuti Machmudah S, Winardi S, Manalu LP, Atmaji G, Widodo WE, Hartono LK, Komariyah K, Alfa MN, Kurniasari I. (2023). The effect of roasting Toraja arabica coffee with a fluidized roaster on the antioxidant and proximate content. IOP Conference Series: Earth and Environmental Science, 1182(1), 012076. doi:10.1088/1755-1315/1182/1/012076
Aung Moon S, Wongsakul S, Kitazawa H, Kittiwachana S, Saengrayap R. (2024). Application of ATR-FTIR for green Arabica bean shelf-life determination in accelerated storage. Foods, 13(15), 2331. doi:10.3390/foods13152331
Aung Moon S, Wongsakul S, Kitazawa H, Saengrayap R. (2022). Lipid oxidation changes of Arabica green coffee beans during accelerated storage with different packaging types. Foods, 11(19), 3040. doi:10.3390/foods11193040
Aung Moon S, Wongsakul S, Kitazawa H, Saengrayap R. (2025). Impact of roasting and storage conditions on the shelf stability of Thai Arabica coffee. Journal of Agriculture and Food Research, 22(2025), 102060. doi:10.1016/j.jafr.2025.102060
Barbin DF, Felicio AL de SM, Sun DW, Nixdorf SL, Hirooka EY. (2014). Application of infrared spectral techniques on quality and compositional attributes of coffee: An overview. Food Research International, 61(2014), 23-32. doi:10.1016/j.foodres.2014.01.005
Berbert PA, Queiroz DM, Sousa EF, Molina MB, Melo EC, Faroni LRD. (2001). Dielectric properties of parchment coffee. Journal of Agricultural and Engineering Research, 80(1), 65-80. doi:10.1006/jaer.2000.0689
Cantaragiu AM, Ivan AS, Alexe P, Dragomir Balanica CM, Stoica M. (2020). Effect of ground and roasted parameters on both the microstructure of Arabica coffee beans and coffee infusion - An imagistic study. Journal of Science and Arts, 20(4), 957-968. doi:10.46939/j.sci.arts-20.4-b01
Carré B, Chopard A, Guillet JP, Fauquet F, Mounaix P, Gellie P. (2023). Terahertz nondestructive testing with ultra-wideband FMCW radar. Sensors, 23(1), 187. doi:10.3390/s23010187
Collazos-Escobar GA, Gutiérrez-Guzmán N, Váquiro HA, García-Pérez JV, Cárcel JA. (2025). Analysis of machine learning algorithms for the computer simulation of moisture sorption isotherms of coffee beans. Food and Bioprocess Technology, 18(6), 5419-5430. doi:10.1007/s11947-025-03785-x
Collazos-Escobar GA, Gutiérrez-Guzmán N, Váquiro-Herrera HA, Bon J, Garcia-Perez JV. (2022). Thermodynamic analysis and modeling of water vapor adsorption isotherms of roasted specialty coffee (Coffee arabica L. cv. Colombia). LWT, 160. doi:10.1016/j.lwt.2022.113335
Dippong T, Dan M, Kovacs MH, Kovacs ED, Levei EA, Cadar O. (2022). Analysis of volatile compounds, composition, and thermal behavior of coffee beans according to variety and roasting intensity. Foods, 11(19), 3146. doi:10.3390/foods11193146
Elezović A, Marić A, BišDević A, HadćEiabdić J, Škrbo S, Špirtović-Halilović S, Rahić O, Vranić E, Elezović A. (2021). In vitro pH dependent passive transport of ketoprofen and metformin. ADMET and DMPK, 9(1), 57-68. doi:10.5599/admet.916
Gao Y, Ravan M, Amineh RK. (2023). Near-field imaging of dielectric components using an array of microwave sensors. Electronics, 12(6), 1507. doi:10.3390/electronics12061507
Geng Y. (2024). Mechanism and Examples of Maillard Reaction. International Journal of Food Science and Agriculture, 8(1), 54-58. doi:10.26855/ijfsa.2024.03.008
Ghattas A, Al-Sharawi R, Zakaria A, Qaddoumi N. (2025). Detecting defects in materials using nondestructive microwave testing techniques: A comprehensive review. Applied Sciences, 15(6), 3274. doi:10.3390/app15063274
Grebenteuch S, Kanzler C, Klaußnitzer S, Kroh LW, Rohn S. (2021). The formation of methyl ketones during lipid oxidation at elevated temperatures. Molecules, 26(4), 1104. doi:10.3390/molecules26041104
Grootveld M. (2022). Evidence-based challenges to the continued recommendation and use of peroxidatively-susceptible polyunsaturated fatty acid-rich culinary oils for high-temperature frying practises: Experimental revelations focused on toxic aldehydic lipid oxidation products. Frontiers in Nutrition, 8, 711640. doi:10.3389/fnut.2021.711640
Hilmi NAM, Khan ZI, Rashid NEA, Mahmood MKA, Zakaria NA, Rahim SAEA. (2021). Parametric evaluation of edible oils using microwave non-destructive testing (MNDT) in X-band frequency. IEEE Symposium on Wireless Technology and Applications 2021, 97-102. doi:10.1109/ISWTA52208.2021.9587422
Ikhwan MF, Mansor W, Ismail Khan Z, Mahmood MKA, Bujang A. (2022). Investigation of animal fats using microwave non-destructive testing at X-band. Journal of Electrical & Electronic Systems Research, 21, 84-90. doi:10.24191/jeesr.v21i1.011
International Coffee Organization. (2025). Coffee Market Report (July 2025), International Coffee Organization.
Iriondo-DeHond A, Elizondo AS, Iriondo-DeHond M, Ríos MB, Mufari R, Mendiola JA, Ibañez E, del Castillo MD. (2020). Assessment of healthy and harmful Maillard reaction products in a novel coffee cascara beverage: Melanoidins and acrylamide. Foods, 9(5), 620. doi:10.3390/foods9050620
Jitjaroen W, Chaisri D, Panjai L. (2023). Characterization of active-aroma wheel in contemporary coffee processes via gas chromatography-olfactometry, and sensory perspective. Coffee Science, 18, 1-13. doi:10.25186/.v18i.2059
Jones SB, Sheng W, Or D. (2022). Dielectric measurement of agricultural grain moisture - Theory and applications. Sensors, 22(6), 2083. doi:10.3390/s22062083
Kafarski M, Szypłowska A, Majcher J, Wilczek A, Lewandowski A, Hlaváčová Z, Skierucha W. (2022). Complex dielectric permittivity spectra of rapeseed in the 20 MHz-3 GHz frequency range. Materials, 15(14), 4844. doi:10.3390/ma15144844
Kim S, Chung SW, An HJ, Lim CK, Jeon MK, Jang YJ. (2022). Changes in morphology, total polyphenols, caffeine, and chlorogenic acid in beans of Arabica coffee (Coffea arabica) during roasting. Journal of the Korean Society of Food Science and Nutrition, 51(4), 344-351. doi:10.3746/jkfn.2022.51.4.344
Mitas O, Han D, Struijer B, Willems L, Chatwick T. (2024). Taking pleasure in distinction: Unlocking specialty coffee preference. Journal of Global Business Insights, 9(1), 77-98. doi:10.5038/2640-6489.9.1.1279
Ochoa-Muñoz AF, Peña-Torres JA, García-Bermúdez CE, Mosquera-Muñoz KF, Mesa-Diez J. (2022). On characterization of sensory data in presence of missing values: The case of sensory coffee quality assessment. Revista chilena de ingeniería, 30(3), 564-573.
Okere EE, Arendse E, Nieuwoudt H, Fawole OA, Perold WJ, Opara UL. (2021). Non-invasive methods for predicting the quality of processed horticultural food products, with emphasis on dried powders, juices and oils: A review. Foods, 10(12), 3061. doi:10.3390/foods10123061
Peña Rodríguez G, Vera Barrera R, Mancipe Huérfano DL, Lara González LÁ. (2021). Electromagnetic properties of a magneto-dielectric composed through an algorithm based on the Nicolson-Ross-Weir method. Ingeniería Investigación y Desarrollo, 21(1), 59-69. doi:10.19053/1900771x.v21.n1.2021.13515
Qiram I, Hamidi N, Yuliati L, Nugroho WS, Wardana ING. (2022). The analysis of Si/Al ratio on CGA decomposition in Indonesian traditional kreweng pottery coffee roaster to maximize coffee acidity. Eastern-European Journal of Enterprise Technologies, 4(6), 22-37. doi:10.15587/1729-4061.2022.260258
Razali AS, Supian FL, Al Naim AF, Ayop SK, Azahari NA. (2021). Raman, FTIR, UV-visible and FESEM studies on calix[8]arene embedded multi-walled carbon nanotubes nanocomposites using spin coating technique. Journal of Science and Mathematics Letters, 9(2), 1-8. https://doi.org/10.37134/jsml.vol9.2.1.2021
Ribeiro RC, Mota MFS, Silva RMV, Silva DC, Novaes FJM, da Veiga VF, Bizzo HR, Teixeira RSS, Rezende CM. (2024). Coffee oil extraction methods: A review. Foods, 13(16), 2601. doi:10.3390/foods13162601
Rodrigues S, Fernandes FAN. (2022). Changing ready-to-drink coffee aroma using dielectric barrier discharge plasma. Processes, 10(10), 2056. doi:10.3390/pr10102056
Rodrigues S, Fernandes FAN. (2023). Green chemistry applied to ground coffee volatile compounds modification aiming coffee aroma improvement. Journal of Food Processing and Preservation, 2023, 1-9. doi:10.1155/2023/4921802
Rune CJB, Giacalone D, Steen I, Duelund L, Münchow M, Clausen MP. (2023). Acids in brewed coffees: Chemical composition and sensory threshold. Current Research in Food Science, 6(2023), 100485. doi:10.1016/j.crfs.2023.100485
Saifuddin MFI, Mansor W, Khan ZI, Bujang A, Mahmood MKA, Ghodgaonkar DK. (2022). Investigation of fat contamination using microwave non-destructive testing at X-band. IEEE Symposium on Wireless Technology and Applications, 72-75. doi:10.1109/ISWTA55313.2022.9942780
Ulpathakumbura S, Marikkar N, Jayasinghe L. (2023). FTIR spectral correlation with alpha-glucosidase inhibitory activities of selected leafy plants extracts. International Journal of Plant Based Pharmaceuticals, 3(3), 104-113. doi:10.29228/ijpbp.22
Velasquez S, Peña N, Bohórquez JC, Gutiérrez N. (2018). Determination of the complex permittivity of cherry, pulped, green, and roasted coffee using a planar dielectric platform and a coaxial probe between 0.3 and 6 GHz. International Journal of Food Properties, 21(1), 1332–1343. doi:10.1080/10942912.2018.1490320
Wu H, Viejo CG, Fuentes S, Dunshea FR, Suleria HAR. (2023). The impact of wet fermentation on coffee quality traits and volatile compounds using digital technologies. Fermentation, 9(1), 68. doi:10.3390/fermentation9010068
Xiong Q, Qiao D, Niu M, Xu Y, Jia C, Zhao S, Li N, Zhang B. (2022). Microwave cooking enriches the nanoscale and short/long-range orders of the resulting indica rice starch undergoing storage. Foods, 11(4), 501. doi:10.3390/foods11040501
Zable MAH, Ismail Khan Z, Abdul Rashid NE, Zakaria NAZ, Ibrahim IP, Enche Ab Rahim SA, Mahmood MKA. (2023). Dielectric material measurement method: A review. Journal of Electrical & Electronic Systems Research, 22, 19-28. doi:10.24191/jeesr.v22i1.003
Zhou YR, Effendy S, Zhu J, Petr MT, Cwalina CD, Bazant MZ, Yildiz B, Li J, Short MP. (2023). Coupled effect of water absorption and ion transport in hydrated latex anti-corrosion coatings. Journal of Coatings Technology and Research, 20(1), 187-200. doi:10.1007/s11998
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Copyright (c) 2026 Mohd Khairil Adzhar Mahmood, Megat Syahirul Amin Megat Ali, Zuhani Ismail Khan , Ahmad Ihsan Mohd Yassin , Irmazatussyehdany Buniyamin, Kwan Yeow Tan, Bazilah Baharom, Wanbo Luo

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